This book focuses on one of the most efficient front-end green approaches in nano-film synthesis and deposition-magneto-plasma polymerization. It fosters an understanding of the fundamentals of the plasma deposition process of C and Si-based organic materials. The text also explores many applications of the materials in various environmental conditions, including biocompatibility, corrosion resistance, electrical insulation failure prevention, durable bonds between rare metal wires and insulation materials, and interfacial engineering utilizing unique nano-film interlayers.